GOST 12340-81
GOST 12340−81 Palladium bullion. Specifications (with Amendments No. 1, 2, 3)
GOST 12340−81
Group W51
INTERSTATE STANDARD
PALLADIUM BULLION
Specifications
Palladium in ingots. Specifications
GST 17 5140
Date of introduction 1983−01−01
INFORMATION DATA
1. DEVELOPED AND INTRODUCED by the Ministry of nonferrous metallurgy of the USSR
2. APPROVED AND put INTO EFFECT by Decision of the USSR State Committee for standards from
Change No. 3 adopted by the Interstate Council for standardization, Metrology and certification (Protocol No. 12, 21.11.97)
The adoption of the changes voted:
The name of the state |
The name of the national authority standardization |
The Republic Of Azerbaijan |
Azgosstandart |
The Republic Of Armenia | Armastajad |
The Republic Of Belarus | Gosstandart Of The Republic Of Belarus |
Georgia | Gosstandart |
The Republic Of Kazakhstan | Gosstandart Of The Republic Of Kazakhstan |
The Kyrgyz Republic | Kyrgyzstandard |
The Republic Of Moldova | Moldovastandart |
Russian Federation | Gosstandart Of Russia |
The Republic Of Tajikistan | Tajikstandart |
Turkmenistan | The MDCSU «Turkmenstandartlary" |
The Republic Of Uzbekistan | Standards |
Ukraine |
Gosstandart Of Ukraine |
3. REPLACE GOST 12340−66
4. REFERENCE NORMATIVE AND TECHNICAL DOCUMENTS
The designation of the reference document referenced |
The number of the paragraph, subparagraph |
GOST 2789−73 | 1.3 |
GOST 9347−74 |
4.3 |
GOST 12225−80 |
3.4 |
5. Limitation of actions taken by Protocol No. 3−93 Interstate Council for standardization, Metrology and certification (ICS 5−6-93)
6. EDITION with Amendments No. 1, 2, 3, approved in June 1987, February 1993, April 1998 (IUS 9−87, 9−93, 7−98)
This standard covers refined palladium bullion intended for the manufacture of alloys, chemicals and other purposes, and establishes requirements for affilirovannomu palladium, izgotovleniu for the needs of national economy and for export.
(Changed edition, Rev. N 1, 2).
1. TECHNICAL REQUIREMENTS
1.1. Palladium bullion is manufactured in accordance with the requirements of this standard for technological regulations approved in the prescribed manner.
Palladium in ingots manufactures brands of PDA-0, PDA-1 and PDA-2.
OKP codes for palladium bullion stamps:
PDA-0 — 175141 0004 01;
PDA-1 — 175141 0005 00;
PDA-2 — 17 5141 0006 10.
(Changed edition, Rev. N 2, 3).
1.2. Chemical composition of palladium bullion must conform to the standards specified in the table.
Item |
Chemical composition, % | ||
Brand PDA-0 |
Brand PDA-1 | Brand PDA-2 | |
Palladium, not less |
99,98 | 99,95 | 99,90 |
Platinum, rhodium, iridium, ruthenium (amount) |
0,015 | 0,025 | 0,050 |
Gold |
0,002 | 0,005 | 0,010 |
Lead |
0,002 | 0,005 | 0,005 |
Iron |
0,003 | 0,005 | 0,020 |
Silicon |
0,002 | 0,005 | 0,005 |
Tin |
0,001 | 0,001 | 0,005 |
Aluminium |
0,002 | 0,005 | 0,005 |
Antimony |
0,002 | 0,010 | 0,050 |
Silver |
0,002 | 0,003 | - |
Magnesium |
0,002 | 0,005 | - |
Zinc |
0,002 | 0,003 | - |
Copper |
0,010 | 0,020 | - |
Nickel |
0,001 | 0,002 | - |
Notes:
1. Mass fraction of silver, magnesium, zinc, copper, Nickel Marche PDA-2 is not rated but is determined by the manufacturer for the accumulation of statistical data.
2. By agreement with the consumer allowed the expansion of the number of determined elements, not shown in the table, and the establishing of norms determined by the method of the manufacturer.
1.3. Palladium is manufactured in the form of rectangular bars with a length of (100±3) mm and a width of (65±2) mm.
Weight of the ingot shall be not more than 3.5 kg.
Allowed by agreement between manufacturer and consumer, the production of palladium bullion with other dimensions and mass.
1.2, 1.3. (Changed edition, Rev. N 2).
1.4. The surface of ingots shall be clean and processed by cutting or grinding.
Foreign inclusions are not allowed.
The surface roughness should be not more than 80 µm according to GOST 2789.
Allowed Stripping of individual surface damage. The depth of the denuded areas on the surface of ingots shall not exceed 1 mm.
(Changed edition, Rev. N 1).
2. ACCEPTANCE RULES
2.1. Palladium bullion accepted by the parties. The party must consist of one of palladium melting of the same brand and designed a quality document and specification.
(Changed edition, Rev. N 2).
2.1.1. The document about quality should contain:
— trademark or a trademark and the name of the manufacturer;
— the name of the metal and its brand;
— the batch number;
— mass fraction of palladium, %;
— mass fraction of each admixture;
room specifications;
— the year of issue;
— the stamp of the technical control Department;
— the designation of this standard.
The mass of the party must be not more than 350 kg.
2.1.2. Specification must contain:
— trademark or a trademark and the name of the manufacturer;
— the name of the metal and its brand;
room specifications;
— the batch number;
— the year of issue;
— the numbers of places;
— number of ingots;
the mass of each ingot, g;
— mass fraction of palladium in each ingot, %;
— mass fraction of each impurity determined in each ingot, %;
— total weight of batch, g;
— the designation of this standard.
2.1.1,
2.2. Control of surface quality and dimensions are subjected to every ingot of the party.
2.3. To check the chemical composition of palladium sampled from each ingot of the party.
2.4. If unsatisfactory results of the analysis of the chemical composition of at least one of the indicators it is carried out re-tests on twice the number of samples taken from the same batch.
The results of repeated tests apply to the entire party.
3. TEST METHODS
3.1. Control of surface quality of ingots of palladium is carried out visually without the use of magnifying devices.
3.2. Size control is carried out measuring tools that provide required accuracy.
3.3. To check the chemical composition of the palladium ingot from each batch sampled in the form of chips no larger than 1 mm.
The mass of the finished sample from the batch shall be not less than 60 g.
Allowed the selection of the sample prepared from the melt with obtaining tablets or cores for spectral analysis.
The shelf life of the samples three months from the date of dispatch of the products to the consumer.
(Changed edition, Rev. N 2).
3.4. Analysis of the chemical composition of palladium is carried out according to GOST 12225.
3.5. The weight of ingots is carried out by weighting according to normative-technical documentation.
4. MARKING, PACKAGING, TRANSPORTATION AND STORAGE
4.1. The front surface of each ingot is applied to the seal, which shall contain the following details:
— trademark of the manufacturer (in the upper left corner);
number (code) of the ingot (under the trademark);
— state symbols manufacturer in Russian or English language, located in the ellipse (lower left corner);
the symbol «Pd» (upper right corner);
— mass fraction of palladium % (under the symbol);
weight of ingot, g or (in the lower right corner).
Permitted additional stigma.
(Changed edition, Rev. N 3).
4.2. Palladium bullion intended for export, Packed in wooden crates or boxes made of other materials, accompanied by documentation in accordance with the order of foreign trade enterprises.
(Changed edition, Rev. N 2).
4.3. Ingots of palladium is Packed in wooden boxes according to normative-technical documentation, pasted inside the foam or the soft cloth of synthetic fiber or metal containers with wooden shells according to normative-technical documentation.
Bars in the containers placed in rows along the height of the wooden shell. Between the horizontal rows of the bars is placed a strip of cardboard according to GOST 9347.
Each box or container sealed with a seal: shop-manufacturer and the technical control Department of the manufacturer.
The seals on the boxes must be suspended through the hole through the bolt after the nut is wrapped up and needs to get out of the groove on the lid of the box. Containers sealed cover locking slots.
4.4. On each box or container and label with the number of specifications and numbers.
4.5. Storage and transportation of ingots is carried out in accordance with the requirements of the Federal financial bodies.
(Changed edition, Rev. N 2, 3).