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GOST 12766.4-90

GOST 12766.4−90 graded rolled steel of precision alloys of high electric resistance. Specifications (with Change No. 1)

GOST 12766.4−90
Group В32

INTERSTATE STANDARD

GRADED ROLLED STEEL OF PRECISION ALLOYS OF HIGH ELECTRIC RESISTANCE

Specifications

Graded rolled steel of precision alloys of high electric resistance. Specifications

OKP 09 6600*
______________
* See notes of FGUP «STANDARTINFORM».

Date of introduction 1991−01−01

INFORMATION DATA

1. DEVELOPED AND INTRODUCED by the Ministry of metallurgy of the USSR

DEVELOPERS

V. I. Matorin, V. V. Sosnin, And V. T. Ababkov, L. L. Zhukov, A. A. Rivkin, M. E. Sopova, M. A. Zinoviev

2. APPROVED AND put INTO EFFECT by Decision of the USSR State Committee on management of quality and standards from 12.02.90 N 187

The change in N 1 taken by the Interstate Council for standardization, Metrology and certification (Protocol № 7 from 26.04.95)

Was the Technical Secretariat of MGS N 1616

The adoption voted:

The name of the state
The name of the national authority
standardization
The Republic Of Belarus
Gosstandart Of Belarus
Russian Federation
Gosstandart Of Russia
Ukraine
Gosstandart Of Ukraine

3. REPLACE GOST 12766.4−77

4. REFERENCE NORMATIVE AND TECHNICAL DOCUMENTS

The designation of the reference document referenced
The number of the paragraph, subparagraph
GOST 166−89
3.2
GOST 427−75
3.2
GOST 2216−84
3.2
GOST 2419−78
3.7
GOST 2590−88
1.2.2
GOST 6507−90
3.2
GOST 7229−76
3.4
GOST 7470−92
3.3
GOST 7502−89
3.2
GOST 7565−81
3.1
GOST 7566−94
1.4.1, 1.5.1, 2.6, 4.1.2
GOST 10446−80
3.8
GOST 10994−74
1.3.1
GOST 12344−88
3.1
GOST 12345−88
3.1
GOST 12346−78
3.1
GOST 12347−77
3.1
GOST 12348−78
3.1
GOST 12350−78
3.1
GOST 12352−81
3.1
GOST 12356−81
3.1
GOST 12357−84
3.1
GOST 12364−84
3.1
GOST 12365−84
3.1
GOST 12766.1−90
1.3.9
GOST 15150−69
4.1.1
GOST 22411−77
1.2.2
GOST 24597−81
4.1.2
GOST 28473−90
3.1

5. Limitation of actions taken by Protocol No. 5−94 of the Interstate Council for standardization, Metrology and certification (ICS 11−12−94)

6. The re-release (December 1998) with amendment No. 1, approved in February 1996 (IMS 5−96)

The re-release (as of November 2008)
______________
* See notes of FGUP «STANDARTINFORM».


This standard applies to hot-rolled steel bars of circular cross-section of precision alloys with high electrical resistance, designed for the manufacture of heating elements and outlet connections.

1. TECHNICAL REQUIREMENTS

1.1. Long products must be manufactured in accordance with the requirements of this standard.

1.1.1. Long products classification:

— delivery:

Hanks — circle;

bars — round (bar);

— the variation of electric resistance of 1 m of rental:

usual quality — 1;

high quality PC;

— standardized indicators:

bars and rods of alloy with a normalized tenacity — A;

bars and rods, of alloy without normalized survivability.

1.2. Basic parameters and dimensions

1.2.1. Depending on the brand of alloy limits rolled sections shall be as given in table.1.

Table 1

Grade Diameter, mm
rod
roll
H15YU5, KHN20JUS
8−30 8−12
KH23JU5, KH23JU5T, KH27JU5T, KHN70JU-N
8−25 8−12
H15N60-H, CR20NI80-H
8−16 8−12

1.2.2. Bars in size, shape and limit deviations should correspond to GOST 2590* normal accuracy of rolling.
_______________
* On the territory of the Russian Federation the document is not valid. Standards 2590−2006. — Note the manufacturer’s database.

On agreement between the consumer and the manufacturer is allowed to produce long products in size, shape and limit deviations in accordance with GOST 22411.

Examples of symbols:

Rolled steel, in coils, with a diameter of 10 mm ordinary quality of grade H15N60-H:

The range 10−1-H15N60-H GOST 12766.4−90


Same rods, 10 mm in diameter of high quality, with a normalized tenacity of alloy grade KH23JU5T:

Circle (bar) 10-PK-A-KH23JU5T GOST 12766.4−90

1.3. Features

1.3.1. The chemical composition of the alloys H15YU5, KHN20JUS, KH23JU5, KH23JU5T, KH27JU5T, KHN70JU-N, H15N60-H, CR20NI80-H should correspond to GOST 10994.

1.3.2. Rolled steel in coils are made in soft annealed condition; in bars without heat treatment. Is permitted to manufacture bars in annealed condition. By agreement between manufacturer and user is allowed to produce long products with etched surface.

1.3.3. Electrical resistance of 1 m long steel in the soft state must conform to the standards given in table.2.

Table 2

Grade Electrical resistance of 1 m Ohm, rolled diameter, mm
8,0
9,0 10,0 11,0 12,0
normal quality increase
high quality
normal quality increase
high quality
normal quality increase
high quality
normal quality increase
high quality
normal quality increase
high quality
H15YU5 0,0233 — 0,0297
0,0244 — 0,0286
0,0185 — 0,0235
0,0193 — 0,0227
0,0150 — 0,0190
0,0156 — 0,0184
0,0120 — 0,0150
0,0124 — 0,0146
0,0101 — 0,0129
0,0106 — 0,0124
KH23JU5 0,0242 — 0,0308
0,0253 — 0,0297
0,0191 — 0,0243
0,0200 — 0,0235
0,0154 — 0,0196 0,0161 — 0,0189 0,0128 — 0,0162 0,0133 — 0,0157 0,0106 — 0,0134 1,0110- 0,0130**
KH23JU5T 0,0250 — 0,0318
0,0261 — 0,0307
0,0196 — 0,0250
0,0205 — 0,0241
0,0158 — 0,0203 0,0167 — 0,0195 0,0131 — 0,0157 0,0137 — 0,0161 0,0110 — 0,0140 0,0115 — 0,0135
KH27JU5T 0,0255 — 0,0325
0,0267 — 0,0313
0,0201 — 0,0255
0,0210 — 0,0246
0,0162 — 0,0206
0,0169 — 0,0199
0,0134 — 0,0170
0,0140 — 0,0164
0,0113 — 0,0143
0,0118 — 0,0138
KHN20JUS* 0,0183 — 0,0233
0,0191 — 0,0255
0,0144 — 0,0184
0,0151 — 0,0177
0,0117 — 0,0149
0,0122 — 0,0144
0,0096 — 0,0122
0,0100 — 0,0118
0,0081 — 0,0103
0,0085 — 0,0100
H15N60-H CR20NI80-H
0,0207 — 0,0263
0,0216 — or 0.0254
0,0163 — 0,0207
0,0170 — 0,0200
0,0132 — 0,0168 0,0138 — 0,0162 0,0110 — 0,0140 0,0115 — 0,0135 0,0090 — 0,0110 0,0092 — 0,0108
KHN70JU-N
0,0230 — 0,0290
0,0244 — 0,0286
0,0185 — 0,0235
0,0193 — 0,0227
0,0150 — 0,0190
0,0156 — 0,0184
0,0124 — 0,0154
0,0128 — 0,0150
0,0102 — 0,0130
0,0107 — 0,0125

_______________
* Standards are not a sign of rejection to 01.01.97. Definition of necessary.

** The text of the document matches the original. — Note the manufacturer’s database.



(Changed edition, Rev. N 1).

1.3.4. The variation of electrical resistance of 1 m within a coil should not exceed 6%.

1.3.5. The persistence of the alloys tested according to the method G, for rolled steel in coils should conform to the standards given in table.3.

Table 3

Grade Test temperature, °C
Vitality, h, not less
H15YU5 1150
120
KH23JU5 1250
80
KH23JU5T 1300
70
KH27JU5T 1300
80
H15N60-H 1150
150
CR20NI80-H 1200
160
KHN20JUS 1150
100
KHN70JU-N 1200
100

Notes:

1. The survivability of the alloy grade KHN20JUS is not a rejection indication to the accumulation of statistical data. Definition of necessary.

2. Bars with a diameter of from 8.0 to 12.0 mm inclusive of alloys with a normalized vitality produce on demand of the consumer.



(Changed edition, Rev. N 1).

1.3.6. (Deleted, Rev. N 1).

1.3.7. The surface of rolled products shall be free from cracks, flaws. Permitted defects such as scratches, fingerprints and individual small prisoner and sunsets with a depth not exceeding half of the total limit deviation for diameter.

By agreement between manufacturer and consumer requirements to the surface quality should match the samples, agreed in the prescribed manner.

1.3.8. Elongation of long-rolled steel in coils should conform to the standards given in table.5.

Table 5*

_______________

* Table.4. (Deleted, Rev. N 1).

GradeГОСТ 12766.4-90 Прокат сортовой из прецизионных сплавов с высоким электрическим сопротивлением. Технические условия (с Изменением N 1)

Elongation ГОСТ 12766.4-90 Прокат сортовой из прецизионных сплавов с высоким электрическим сопротивлением. Технические условия (с Изменением N 1), %, not less

H15YU5 16
KHN20JUS 20
KH23JU5, KH23JU5T 12
KH27JU5T 10
H15N60-H, CR20NI80-H 20
KHN70JU-N
15

1.3.9. The weight of one coil of rolled products should conform to the standards given in table.6.

Table 6

Diameter, mm Weight, kg, not less
normal reduced
From 6,0 to 7,0 incl.
20,0 10,0
SV. 7,0 " 9,0
" 30,0 10,0
" 9,0 " 12,0 " 40,0 10,0



The party allowed Hanks to the reduced mass of not more than 15% (by weight).

By agreement between manufacturer and consumer produce bags of different mass.

1.3.10. Correction factors for calculating changes in electrical resistance depending on temperature, the estimated service life is given in annexes 1 and 2; physical and mechanical properties of alloys, the maximum operating temperature are given in appendices 4−6 GOST 12766.1.

1.4. Marking

1.4.1. Labeling — according GOST 7566.

1.5. Packaging

1.5.1. Packaging according to GOST 7566 with additions.

1.5.1.1. Long products must be in rolls or bundles of skeins or rods. Skein must consist of one segment.

1.5.1.2. The outer diameter of a coil should be no more than 1200 mm, internal — not less than 180 mm.

1.5.1.3. Weight of cargo must not exceed when mechanized loading and unloading in open vehicles 5000 kg, indoor — 1250 kg.

2. ACCEPTANCE

2.1. Long products take parties. The party must consist of one metal bottoms, same size and must be issued a document about quality that contains:

— trademark or name, or the name and trademark of manufacturer;

— the symbol of long products;

— the weight of the batch;

— test results*;

— chemical composition of the alloy.
____________________
* Document the quality in the line «results of tests of the survivability of» record «factory guarantee».


(Changed edition, Rev. N 1).

2.2. To check the quality of rolled products from the party taken:

— to determine the chemical composition of one sample from the melt;

— to determine the size, surface quality, weight 100% product;

— to determine the variation of electrical resistance of 1 m within a coil, an electric resistance of 1 m, relative elongation three coils (of wire). If there are more than three coils (bars) from each coil (bar) select three of the sample;

— to determine the survivability of a single sample of weight, enough to make at least 5 m wire with a diameter of 0.8 m.

2.3. Control of the variation of electrical resistance of 1 m within the same roll, the manufacturer conducts periodic, but not less than once per year.

2.4. The chemical composition of the alloys is certified by a document of quality issued by the company, smelting the metal.

2.5. The tenacity of alloys is certified according to a quality document issued by the company, izgotovlyayuschei wire, according to test results of other heats of the same cycle of melting.

Allowed to the manufacturer of rolled steel to ensure the survivability of the stability of manufacturing technology.

(Changed edition, Rev. N 1).

2.6. If unsatisfactory test results of at least one indicator of a re-test is carried out according to GOST 7566.

3. CONTROL METHODS

3.1. Sampling for chemical analysis is carried out according to GOST 7565.

Chemical composition of alloys determined according to GOST 28473, GOST 12344−12348 GOST, GOST 12350, 12352 GOST, GOST 12356, 12357 GOST, GOST 12364, 12365 GOST or other methods providing the required accuracy of the analysis.

(Changed edition, Rev. N 1)

3.2. The diameter and shape of the rolled section check caliper according to GOST 166, micrometer according to GOST 6507 or staples according to GOST 2216 in two mutually perpendicular directions of the same cross-section in at least three places.

The length of the rods check metal ruler according to GOST 427 or measuring tape according to GOST 7502.

3.3. The surface quality is checked visually. If necessary, the depth of the defect determine the micrometer depth gauge according to GOST 7470 or other tool, to ensure the necessary accuracy, or Stripping prior to the removal of the defect.

The location of the defect cleaned with sandpaper or a file with further comparative dimension to the stripped and unstripped areas.

3.4. Electrical resistance of long products is determined according to GOST 7229 with the use of instruments of accuracy class not worse than 0,05.

3.5. Mass of a coil is determined on the scales, ensuring the necessary measurement accuracy.

3.6. To determine the variation of electrical resistance within the coil to measure the electric resistance at the beginning and end of the strand and the difference between them relates to the arithmetic mean of the obtained values.

3.7. The tenacity of alloys is determined according to GOST 2419 method G, until it fails.

(Changed edition, Rev. N 1).

3.8. Elongation is determined according to GOST 10446 on samples with an estimated length of 100 mm.

3.9. For each type of testing shall be one sample from each selected coil or bar.

4. TRANSPORTATION AND STORAGE

4.1. Transportation and storage GOST 7566 with additions.

4.1.1. Storage conditions of long products up to 1 month — 3ЖЗ according to GOST 15150, for more than 1 months — 1L according to GOST 15150.

4.1.2. When transporting long products produced consolidation packages in accordance with GOST 24597.

The uld (link in links) according to GOST 7566.

(Changed edition, Rev. N 1).

5. MANUFACTURER’S WARRANTY


The manufacturer guarantees product compliance with the requirements of this standard while complying with the storage conditions. A storage warranty period — three years from the date of manufacture for rolled alloys grades KHN20JUS, H15N60-H, CR20NI80-H, KHN70JU-N two years from the date of manufacture for grades H15YU5, KH23JU5, KH23JU5T, KH27JU5T.

ANNEX 1 (reference). Correction factors for calculating changes in electrical resistance depending on temperature

ANNEX 1
Reference



Table 7

Mark
alloy

The values of the correction factor ГОСТ 12766.4-90 Прокат сортовой из прецизионных сплавов с высоким электрическим сопротивлением. Технические условия (с Изменением N 1)at the temperature of heating, °C

20 100 200 300 400 500 600 700 800 900 1000 1100 1200 1300 1400
H15n60-H
1,000 1,013 1,029 1,046 1,062 1,074 1,083 1,083 1,089 1,097 1,105 1,114 - - -
H15YU5
1,000 1,004 1,014 1,025 1,041 1,062 1,090 1,114 1,126 1,135 1,14 - - - -
KH23JU5, KH23JU5T
1,000 1,002 1,007 1,013 1,022 1,036 1,056 1,063 1,067 1,072 1,076 1,079 1,080 1,083 1,086
KH27JU5T
1,000 1,002 1,005 1,010 1,015 1,025 1,030 1,033 1,035 1,040 1,040 1,041 1,043 1,045 -
CR20NI80-H
1,000 1,006 1,015 1,022 1,029 1,032 1,023 1,016 1,015 1,017 1,025 1,033 1,040 - -
KHN70JU-N
1,000 1,004 - - - 1,052 1,053 1,036 1,015 1,016 1,016 1,023 1,031 - -
KHN20JUS
1,000 1,035 1,075 1,110 1,145 1,18 1,21 Of 1.23 1,25 1,27 1,29 Of 1.31 - - -


Note. The electrical resistance at room temperature (ГОСТ 12766.4-90 Прокат сортовой из прецизионных сплавов с высоким электрическим сопротивлением. Технические условия (с Изменением N 1)) was determined for each alloy after heating the sample to temperatures above 600 °C and cooling with the furnace. In this case, the electric resistance (ГОСТ 12766.4-90 Прокат сортовой из прецизионных сплавов с высоким электрическим сопротивлением. Технические условия (с Изменением N 1)) above governed by this standard; for grade H15N60-H — 3%, for grades KHN70JU-N, CR20NI80-H — 5% and below, governed by this standard: for grade H15YU5 — 2%; for grades KH23JU5, KH23JU5T, KH27JU5T — 4%; alloy grade KHN20JUS.

ANNEX 2 (informative). The estimated lifespan of long products made of alloys with high electric resistance when working as a heater

ANNEX 2
Reference



Table 8

Grade
Diameter, mm Temperature, °C Service life, h
not less than
KHN70JU-N 6.0 and more 1200
6000
CR20NI80-H 1200
H15N60-H 1125
KHN20JUS 1100
KH23JU5 1200
H15YU5 1000
KH23JU5T

KH27JU5T
1300


Notes:

1. The values of life given according to all-Union scientific-research Institute of electrothermal equipment.

2. The grades KH23JU5 and H15YU5 is not recommended to use as heaters.

3. The useful life is determined in an atmosphere of air on the zig-zag samples with the height of the ridge to the iron-chrome-aluminum alloy is not more than 200 mm and for nickelchromium alloy is not more than 300 mm bending Radius at least one radius of the wire, the pitch of the ridge from 100 to 140 mm. the Samples are placed inside the chamber with thermal insulation, the heating is conducted by passing current. Specific surface load ГОСТ 12766.4-90 Прокат сортовой из прецизионных сплавов с высоким электрическим сопротивлением. Технические условия (с Изменением N 1).

NOTES OF FGUP «STANDARTINFORM»


1 On the first page to Supplement code: ISS 77.140.50 (index «National standards», 2008).

2 Information data. Reference normative and technical documents:

GOST 7502−89 replaced by GOST 7502−98;

GOST 12344−88 replaced by GOST 12344−2003;

GOST 12345−88 replaced by GOST 12345−2001 (ISO 671−82, ISO 4935−89)