GOST 745-2003

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  ГОСТ 745-2003

GOST 745−2003 aluminium Foil for packaging. Specifications

GOST 745−2003

Group В53

INTERSTATE STANDARD
ALUMINIUM FOIL FOR PACKING

Specifications

Aluminium foil for packing. Specifications

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Text Comparison 745−2003 GOST with GOST 745−2014 see the link.
— Note the manufacturer’s database.
____________________________________________________________________

ISS 77.120*
GST 18 1119
______________
* According to the official website of Rosstandart
OKS 77.150.10, here and hereafter. -
Note the manufacturer’s database.

Date of introduction 2004−09−01

Preface

1 DEVELOPED by the Russian Federation, Technical Committee for standardization TC 106 «Tsvetmetprokat», scientific-research and design Institute for alloys and processing of nonferrous metals (JSC «Institute tsvetmetobrabotka»)

SUBMITTED by the Technical Secretariat of the Interstate Council for standardization, Metrology and certification

2 ADOPTED by the Interstate Council for standardization, Metrology and certification (Protocol No. 23 dated 22 may 2003), was a standards Bureau MGS N 4436

The adoption voted:

The name of the state	The name of the national authority for standardization
Azerbaijan	Azstandart
The Republic Of Armenia	Armastajad
The Republic Of Belarus	Gosstandart Of The Republic Of Belarus
Georgia	Gosstandart
Kazakhstan	Gosstandart Of The Republic Of Kazakhstan
The Kyrgyz Republic	Kyrgyzstandard
The Republic Of Moldova	Moldovastandart
Russian Federation	Gosstandart Of Russia
The Republic Of Tajikistan	Tajikstandart
Turkmenistan	The MDCSU «Turkmenstandartlary"
Uzbekistan	Uzstandard

3 Resolution of the State Committee of the Russian Federation for standardization and Metrology on January 20, 2004 N 22-St interstate standard GOST 745−2003 introduced directly as a national standard of the Russian Federation from September 1, 2004

4 REPLACE GOST 745−79

AMENDED, published in the IUS N 9, 2004

An amendment made by the manufacturer of the database.

1 Scope

This standard applies to cold-rolled aluminum foil, designed for packaging of foods, drugs, medical devices, cosmetic products industry, as well as for the production of packaging materials based on aluminum foil.

The product safety requirements set out in 5.3, 5.4, 6.3, 7.4, 7.5.

2 Normative references

The present standard features references to the following standards:

GOST 166−89 (ISO 3599−76) Calipers. Specifications

GOST 427−75 Rulers measuring metal. Specifications

GOST 2768−84 Acetone. Specifications

GOST 2991−85 wooden disposable Boxes for loads up to 500 kg. General specifications

The Wire GOST 3282−74 General purpose low carbon steel. Specifications

GOST 3560−73 package steel Strip. Specifications

GOST 4381−87 Micrometers lever. General specifications

GOST 4784−97 Aluminum and aluminum deformable alloys. Brand

GOST 5556−81 Wool medical hygroscopic. Specifications

GOST 6507−90 Micrometers. Specifications

GOST 6709−72 distilled Water. Specifications

GOST 7376−89 corrugated Cardboard. General specifications

GOST 7502−98 metallic measuring tape. Specifications

GOST 8828−89 base Paper and paper double-layer waterproof packaging. Specifications

GOST 8981−78 Esters of ethyl and normal butyl acetic acid technical. Specifications

GOST 9078−84 flat Pallets. General specifications

GOST 9557−87 flat wooden Pallet size 800x1200 mm. specifications

GOST 10198−91 Boxes, wooden, for loads weighing over 200 up to 20000 kg. General specifications

GOST 10354−82 polyethylene Film. Specifications

GOST 11069−2001 primary Aluminium. Brand

GOST 12697.2−77 Aluminum. Methods for determination of magnesium

GOST 12697.3−77 Aluminum. Methods for determination of manganese

GOST 12697.6−77 Aluminum. Method for determination of silicon

GOST 12697.7−77 Aluminum. Methods of iron determination

GOST 12697.8−77 Aluminum. Methods for determination of copper

GOST 12697.9−77 Aluminum. Methods for determination of zinc

GOST 12697.10−77 Aluminum. Method of determining titanium

GOST 14192−96 Marking of cargo

GOST 15467−79 quality Control of products. Basic concepts. Terms and definitions

GOST 18477−79 Containers are universal. The types, basic parameters and dimensions

GOST 21140−88 Tara. System sizes

GOST 24231−80 non-ferrous metals and alloys. General requirements to selection and preparation of samples for chemical analysis

GOST 24597−81 the packaged goods. Basic parameters and dimensions

GOST 26663−85 transport Packs. Formation with the use of packaging. General technical requirements

GOST 28798−90 Head of the measuring spring. General specifications

3 Types and designations

3.1 as the treated surface of the foil is divided into the following types:

FY — smooth;

FL — lacquered on one side;

FLL — lacquered or both sides;

FTL — patent by heat-sealing;

FO — painted with colored lacquers or paints;

FP — printing;

FPL — with printing on front side and patent on the back side;

FPTL — printed on the front side and a heat-sealing lacquer on the reverse side;

FLTL — with the ground under printing on the front side and a heat-sealing on the reverse side.

If the foil is subjected to a further embossing, to the above symbols, you must add the designation «TS».

4 Assortment

4.1 foil Thickness and limit deviation on thickness shall be as specified in table 1.

Table 1 — Thickness of the foil and limit deviations for thickness

In millimeters

Foil thickness	Limit deviation on thickness
	Normal accuracy	Improved accuracy	High precision
0,006 0,007 0,008 0,009 0,010 0,011	±0,001	-	-
0,012 0,013 0,014 0,015	+0,001 -0,002	-0,002	-
0,016 0,017 0,018 0,019 0,020	±0,002	+0,001 -0,002	-
0,025 0,030 0,035	±0,003	+0,001 -0,003	-
0,040 0,045	±0,004	+0,002 -0,004	+0,002 -0,003
0,050 0,055	±0,005	+0,003 -0,005	+0,002 -0,004
0,060 0,065 0,070	±0,006	+0,004 -0,006	+0,003 -0,005
0,080 Of 0.085 0,090	±0,007	+0,003 -0,008	+0,003 -0,006
0,100 0,120 0,150	+0,005 -0,010	+0,004 -0,010	+0,004 -0,008
0,180 0,200	±0,015	+0,005 -0,015	+0,005 -0,012
Notes 1 can be manufactured in foil of thickness in excess of 0.200 to 0.240 inch mm with maximum deviation in thickness: normal accuracy — ±0,015; increased accuracy — +0,005 -0,012. 2 foil Thickness specified before applying paint coatings. The thickness of the paint coating on the foil is governed by the requirements of the consumer in accordance with the scope. 3 the Surface density of the foil at a nominal thickness is for reference only and is given in Appendix A.

4.2 Foil made of a width from 15 to 1500 mm. the Gradation width of the foil must be 5 mm for widths up to 500 mm 10 mm — at width more than 500 mm.

The width of the foil and maximum deviations in width of all types should correspond to those in table 2.

Table 2 — the Width of the foil and limit deviations on width

In millimeters

Width	Limit deviation width
From 15 to 100 incl.	±0,5
SV. 100 «500 «	±1,0
«500» 750 «	±1,5
«750» 1500 «	±2,0

4.3 Foil of all kinds should be wound on a metal sleeve (spool) inside diameter of 34−36, 50−52, 68−70, 75−77 150−153 mm. or the size of the sleeve is determined by agreement between manufacturer and consumer. Sleeve length should be equal to the nominal width of the foil. Permissible deviations on length of sleeve — ±2.0 mm.

By agreement with the consumer allowed to apply the sleeve length exceeding the nominal width of the foil.

In the case where the length of the bushing exceeds the nominal width of the foil, the protruding ends of the sleeve must be the same. The difference of the lengths of the protruding ends of the bushings should be no more than 4 mm.

By agreement with the consumer allowed to wind the foil on the non-metallic sleeve.

4.4 Foil must be wound in coils outer diameter is 100−800 mm. deviation from the nominal roll diameter is ±10%.

Allowed winding foil coils of smaller diameter, but not less than 1.5 times the size of the inner diameter of bushing not more than 10% of the batch weight.

By agreement with the consumer allowed to limit the outer diameter of the coil smaller or limit the weight of one roll.

In coordination with the consumer the outer diameter of coils can be increased.

Legend foil tabulated according to the scheme:

Use the following abbreviations:

— precision manufacturing:

normal — N,

increased — P,

high.

— status:

soft — M

solid — T.

Examples of symbols:

The smooth foil thickness of 0.050 mm, width 100 mm, normal precision manufacturing, aluminium brand A5, soft:

Foil FG 0,050х100 N A5 M GOST 745−2003

Smooth embossed foil with a thickness of 0.050 mm, width 100 mm, normal precision manufacturing, aluminium brand A5, soft:

Foil Fgts 0,050х100 N A5 M GOST 745−2003

5 Technical requirements

5.1 Foil manufactured in accordance with the requirements of this standard for technological regulations approved in the prescribed manner. Foil made from aluminum and aluminum alloys brands: AD, AD0 and AD1 with the chemical composition according to GOST 4784; A6, A5 and A0 with the chemical composition according to GOST 11069; AZH0,6, AZH0,8, AZH1 with the chemical composition shown in table 3, 8011, 8011A, 8111, 1145 1050 and with the chemical composition shown in table 4.

Table 3 — Chemical composition aluminium and aluminium alloys

Mass fraction, %
The main element		Impurity, not more than
Grade aluminum and aluminum alloy	Al aluminium	Fe iron	Si silicon	Si copper	Zn zinc	Ti Titan	Other impurities (each)	Just
AZH0,6	99,0−99,2	0,40−0,60	0,20	0,01	0,06	0,03	0,03	0,40
AZH0,8	98.70 a barrel-98,90	0,60−0,80	0,30	0,02	0,06	0,03	0,03	0,50
AZH1	98,35−98,55	0,95−1,15	0,20	0,01	0,06	0,03	0,05	0,50

Table 4 — Chemical composition aluminium and aluminium alloys

Mass fraction, %
The main element			Impurity, not more than
Grade aluminum and aluminum alloy	Al aluminium	Fe iron	Si silicon	Si copper	Mn manganese	Mg magnesium	Zn zinc	Ti Titan	Other impurities (each)
1145	Not less than from 99.45	No more 0,55 (Fe + Si)		0,05	0,05	0,05	0,05	0,03	0,03
1050	Not less than a 99.50	Not more than 0.40	Not more than 0.25	0,05	0,05	0,05	0,07	0,05	0,03
8011	The rest	0,6−1,0	0,5−0,9	0,10	0,20	0,05	0,10	0,08	0,05
8011A	The rest	0,5−1,0	0,4−0,8	0,10	0,10	0,10	0,10	0,05	0,06
8111	The rest	0,4−1,0	0,3−1,1	0,10	0,10	0,05	0,10	0,08	0,05

By agreement with the consumer allowed the use of other aluminum alloys permitted by MoH for use in contact with food.

5.2 All materials used for manufacturing the foil according to the present standard must be authorized by national health authorities.

5.3 the Foil should make contact with her model solutions simulating foods, harmful substances in quantities exceeding the established [1] and components: for aluminum — 0,500 mg/l, manganese — 0,100 mg/l, iron — 0,300 mg/l, copper — 1,000 mg/l, zinc — 1,000 mg/l, titanium — 0,100 mg/l and vanadium — 0,100 mg/l.

5.4 Foil should not have a smell, affecting the quality of Packed products.

5.5 All kinds of foil are made in the soft (annealed) or hard (unannealed) condition.

The mechanical properties of the foil are not regulated.

5.6 On the foil should not be extraneous inclusions and surface dirt, folds, tears, nicks, corrosion and stains from faded rolling oil.

Allowed on the surface of the foil prints from rolls, not bringing the foil over the limit deviation on thickness.

On the foil thickness from 0.017 to 0,030 mm permitted small isolated holes visible to the naked eye against the light.

On the foil with thickness less than 0.017 mm micropores and holes is determined in accordance with the method of testing the foil on the porosity contained in Appendix B. Not allowed the accumulation of stroke and the location of the holes on the foil.

Allowed to set the surface quality of the foil, the number and location of through-holes and micropores of the samples agreed between manufacturer and user.

On the surface of soft (annealed) foil is not allowed the presence of residues of the technological lubricant.

On the surface of hard (unannealed) foils allowed the remnants of the technological lubricant.

5.7 colors of the print, as well as drawings of the embossing and printing are samples agreed between manufacturer and user. To conduct prepress user presents a diagram of the orientation of the pattern roll and the original picture made of the photographic method or black ink, not giving rasplava stroke on a white piece of paper, with the layout by color, showing all dimensions, colors, as well as the location and size of the tags under the machines.

5.8 Paint to be coated on the entire surface of the foil in a uniform layer with satisfactory adhesion to the surface of the foil. Unpainted places are not allowed. Not allowed swelling and detachment of the varnish film on the surface of the foil and crack the lacquer coating at the bend.

When covering with foil varnishes and heat-sealing point side of the coating.

Allowed the quality of the varnish coating to determine on the agreed samples.

Additional requirements to the quality of the paint application must be agreed between manufacturer and user.

5.9 1 membossed or printed foil is allowed no more than six sites with an irregular pattern of the embossing or printing size no more than 1 cmeach.

Sticking of the turns of foil after coating or printing is not permitted.

5.10 the Foil should be wound with tension that does not allow displacement of the individual turns of the coil and the loss or displacement of the bushing while turning the coil 90° and 180°.

When winding all kinds of foil on the sleeve allowed the displacement of the coils in the ends of the roll for foil thickness:

— to 0.020 mm inclusively — no more than 1 mm;

— more than 0.020 mm — 2 mm.

The ends of the roll must be free of nicks, dings and dirt.

5.11 throughout the length of the foil roll should be easily unwound, the foil edge must be no significant (GOST 15467) burrs or tears.

Permitted scalloped edge, due to cutting way and disappearing when winding the foil into a roll.

(Amendment. ICS N 9−2004).

5.12 permits one roll of foil with a thickness of 0.014 mm and not less than five breaks, with a thickness of 0.018 to 0.05 mm inclusively — no more than four breaks, of a thickness exceeding 0,05 mm — of no more than three breaks.

6 acceptance Rules

6.1 Foil take parties. The party should consist of a foil of the same species, made of aluminium, same brand, same size, same manufacturing accuracy in thickness, one state and must be issued a document about quality that contains:

is the trademark or name and trademark of manufacturer;

— the name of the country of manufacture;

— legal address of the manufacturer and (or) the seller;

— basic (or functional) purpose, or usage;

— the symbol foil;

— the batch number;

the sign of conformity (for foil, certified);

— the weight of the batch;

— bar code (if available).

The weight of the batch is not limited.

6.2 For inspection and measurement of the foil of all brands from the party take 5% rolls, but at least two.

6.3 For monitoring the presence of the smell of the technological lubricant, dircetory, quality of raskatyvaete and paint film adhesion of the coating to the foil from the party take 5% of the rolls of foil, but at least two.

6.4 For the control of the chemical composition of the foil on the manufacturer carried out the sampling of molten metal from each melting, for the enterprise, the consumer take away one roll from the party.

6.5 If unsatisfactory test results of at least one indicator thereon, a second test of the doubled sample taken from the same batch. The results of repeated testing are spreading to the entire party.

7 control Methods

7.1 For inspection and measurement of the foil from the end of the roll rewind 3 m foil Inspection should be conducted visually without the use of magnifying devices.

7.2 the Thickness of the foil is measured by a measuring head according to GOST 28798 or micrometer according to GOST 6507 or GOST 4381.

The width of the foil is measured by Vernier caliper according to GOST 166, metal ruler according to GOST 427 or metal measuring tape according to GOST 7502.

A lot of the paint coating on the foil is determined according to the method set out in Annex V.

Allowed to use other means of measurement that provides the required accuracy set by the standard.

If there is disagreement monitoring is carried out by means of measurement specified in the standard.

7.3 Selection and preparation of samples for the determination of chemical composition is carried out according to GOST 24231.

Chemical analysis carried out according to GOST 12697.2, 12697.3 GOST, GOST 12697.6, 12697.8 GOST-GOST 12697.10.

Allowed the use of other methods of chemical analysis, which is not inferior in accuracy are listed.

If there is disagreement in the assessment of the chemical composition of the foil analysis is carried out according to GOST 12697.2, 12697.3 GOST, GOST 12697.6-GOST 12697.10.

7.4 Sanitary-chemical studies of finished products is carried out in accordance with the requirements of [1].

7.5 the Presence of odor in the foil is determined organoleptically.

In the case of a dispute, the presence of odor in the foil is determined according to the method of odor determination foil set forth in Annex G.

7.6 Control of presence of technological lubricant on the surface of soft (annealed) and hard (unannealed) foils is carried out by testing the wettability. Method of determining wettability of the foil is set out in Annex D.

7.7 Control of porosity of the foil is carried out according to the method set out in Annex B. For the control take one sample across the width of the foil nominal thickness and a length of 3.5 m in the direction of rolling of each of the selected coil.

7.8 the Quality of raskatyvaete foil is controlled according to the method of determining raskatyvaete foil set forth in Annex E.

(Amendment. ICS N 9−2004).

7.9 the adhesion of the paint coating to the surface of the foil is controlled according to the method set out in Annex J.

Satisfactory adhesion of a paint coating is considered to be the adhesion of the classes A, b, C.

8 Packing, marking, transportation and storage

8.1 Each roll of foil must be wrapped with a paper tape of a width equal to the width of the foil.

Allowed the use of other materials that protect the outer surface of the roll from contamination.

8.2 On each roll of foil must be tagged, indicating:

— trademark or name and trademark of manufacturer;

— the name of the country of manufacturer;

— legal address of the manufacturer and (or) the seller;

— primary (or functional) purpose, or application;

— the legend foil;

— bar code (if available);

— batch number;

— stamp of technical control;

— the mark of conformity (for foil, certified);

— the date of manufacture.

8.3 All kinds of foil is Packed in tight or slatted wooden crates types III-1, III-2 according to GOST 2991 or GOST 10198. Dimensions of boxes — GOST 21140. It is allowed to transport the foil without package in universal containers according to GOST 18477. The floor of the container and the boxes lined with two-layer waterproof packing paper according to GOST 8828 or polyethylene film according to GOST 10354. The same paper or film is available Packed foil.

The rolls of foil up to a thickness of 0.018 mm, inclusive transporterowych in limbo. The coils should slide on steel rods, reinforced between the wooden struts of the container or box.

The rolls of foil with a thickness of more than 0,018 mm are placed in containers or boxes on end or horizontally.

It is possible to stow rolls of foil thickness of 0.014 to 0.200 mm in a box or container on the end. The ends of the rolls must be protected from mechanical damage corrugated cardboard according to GOST 7376.

8.4 By agreement with the consumer allowed other methods of packaging and protection of the rolls of foil from corrosion and mechanical damage, according to its qualities and corrosion properties are not inferior to those listed in 8.3 and ensuring the safety of the quality of the foil during transport.

8.5 Consolidation packages in overpacks carried out in accordance with the requirements of GOST 26663. Packaging is carried out on pallets according to GOST 9557, GOST 9078 wooden or metal pallets according to normative documents approved in the prescribed manner, or without trays using the bricks of height at least 50 mm, with the piping in the longitudinal and transverse directions with wire of diameter not less than 2 mm according to GOST 3282 or tape not less than 0,3х30 mm according to GOST 3560. Fasten the ends: wire — strand minimum 5 turns the ribbon to the castle. Packet size — according to GOST 24597.

8.6 Transport marking under GOST 14192 with the application of manipulation signs: «Protect from moisture», «Fragile. Caution."

For rolls of foil certified conformity mark is applied to each package in close proximity to the trademark of the manufacturer.

8.7 In each container or box shall be attached to packing list stating:

— trademark or name and trademark of manufacturer;

— the name of the country of manufacturer;

— legal address of the manufacturer and (or) the seller;

— primary (or functional) purpose, or application;

— the legend foil;

— bar code (if available);

— the mark of conformity (for foil, certified);

— batch number;

— weight;

— gross mass;

— the number of coils;

— the numbers of packer.

8.8 Foil transporterowych all types of transport in covered vehicles in accordance with cargo carriage regulations applicable to transport of this species.

By agreement with the consumer allowed to transport the foil in the RV without packing in boxes and containers.

8.9 Foil must be stored in accordance with the rules of storage of aluminum foil, is given in Appendix I.

Annex a (informative). The surface density of the foil at a nominal thickness

APPENDIX A
(reference)

Table A. 1

Thickness, mm	Surface density, g/m, for grades
A0, A5, A6, AD, AD0, AD1, AZH0,6, 1050, 1145	AZH0,8, AZH1, 8011, 8011A, 8111
0,006	16,2	16,3
0,007	18,9	19,0
0,008	21,6	21,7
0,009	24,3	24,4
0,010	27,0	27,1
0,011	29,7	29,8
0,012	32,4	32,5
0,013	35,1	35,2
0,014	37,8	37,9
0,015	40,5	40,7
0,016	43,2	43,4
0,017	45,9	46,1
0,018	48,6	48,8
0,019	51,3	51,5
0,020	54,0	54,2
0,025	67,5	67,8
0,030	81,0	81,3
0,035	94,5	94,9
0,040	108,0	108,4
0,045	121,5	122,0
0,050	Of 135.0	135,5
0,055	148,5	149,1
0,060	162,0	162.6 mln
0,065	175,5	176,2
0,070	189,0	189,7
0,080	216,0	216,8
Of 0.085	Of 229.5	At $ 230.4
0,090	243,0	243,9
0,100	: 270.0 cm	271,0
0,120	324,0	325,2
0,150	405,0	406,5
0,180	486,0	487,8
0,200	540,0	542,0
0,240	648,0	650,4
Note — When calculating the surface density of the foil, density aluminium and aluminium alloys A0, A5, A6, AD, AD0, AD1, AZH0,6, 1050 and 1145 estimated to be equal to 2.7 g/cm, and brands AZH0,8, AZH1, 8011, and 8011A 8111 — 2.71 g/cm.

APPENDIX B (mandatory). Test method foil on porosity

APPENDIX B
(required)

This method establishes the procedure for testing the porosity of the foil. This method is applicable for aluminium foil in thickness from 0.006 to 0.030 mm. the essence of the method is that you count the number of long, chaotic, or stroke holes, and pores with a diameter less than 0.020 mm is determined.

Pores is arbitrarily distributed holes in the foil with thickness from 0.006 to 0.020 mm usually round or oval in shape and a maximum diameter of 0.20 mm.

Chaotic hole is a hole with a maximum diameter of more than 0.20 mm, which appear in any area along the entire length of the roll.

Stroke hole is a hole with a maximum diameter of more than 0.20 mm that appear along the entire length of the roll using natural intervals.

B. 1 Instrument

Closed dark room lighting of 20−50 Lux.

Table of translucent frosted glass with lighting.

Fluorescent lamp light of 1000 to 1500 Lux.

Stencil an area of 1 DM.

B. 2 testing

A controlled sample is placed on a light table matte surface up. Cover the area of the light table, not covered by a controlled sample. Carefully looking at the controlled sample at a distance of 0.5 m from the surface of the controlled sample.

The test area chosen as follows.

A — random selection: a sample area of 1 DMis chosen randomly.

B — selection of the worst area: the sample area of 1 DMchoose from the precinct with the highest number of pores.

On a selected area, calculates the number of clusters, the through-holes or prints from the rolls. The micropores of the selected worst plot count through the stencil area of 1 DM. Further, the number multiplied by 100. The results should be expressed in the number of micropores per 1 m.

ANNEX b (mandatory). The method of determining the weight of the lacquer coating on the foil

THE APP
(required)

This method specifies how to measure the mass of coatings on aluminum foil.

B. 1 Apparatus, reagents, materials

Aluminium foil lacquered or painted.

Circular shearing machine for cutting samples or metal pattern area of 10 x 10 cm

Analytical balance.

Ethyl acetate or other solvent type acetone or toluene according to GOST and GOST 8981 2768.

Wool GOST 5556.

Paper napkins.

B. 2 testing

Cut using a circular shearing or template a sample area of 100 cm. Weigh the sample on an analytical balance accurate to the fourth decimal place. Record this result as the weight .

Place the sample on the paper towel, moisten a piece of clean cotton wool with solvent and remove the paint by wiping the surface of the sample soaked in solvent with cotton, while avoiding getting solvent on the other side of the sample. The sample is dried and weighed, record the result as the weight .

A lot of the paint coating , g/m, is calculated by the formula

. (B. 1)

A lot of the paint coating on the second side of the foil is determined similarly: after removing the coatings with a cotton swab dipped in solvent, and drying the foil sample is weighed, record the result as the weight .

The weight of the coating on the second side , g/cm*, is calculated by the formula

. (B. 2)

For the result of the determination accepted the values for the mass of two parallel measurements.

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* Text sootvetstvet the original. — Note the manufacturer’s database

APPENDIX d (mandatory). Method of odor determination foil

APPENDIX D
(required)

This method establishes a test procedure for the smell of foil.

G. 1 Apparatus, reagents, materials

Wide-mouth glass vessels with a height of 10 cm.

Aluminum foil for sealing of glass vessels, decorated in a drying Cabinet at 120 °C for 1 h to remove the abnormal odors.

Rubber rings or good flexible wire for fastening aluminum foil.

Cutter, pattern 10x10 cm or circular shearing.

Drying Cabinet with heater temperature to 150 °C.

G. 2 test Conditions

The test is conducted by the Committee of three employees of quality control Department and laboratory the testing laboratory.

The expert conducting the test, should not use chewing gum, use perfume or other fragrances should not smoke during the test.

Hands must be clean and deodorized. If hands get sweaty, you should wear clean cotton gloves.

For the analysis over the entire width of the roll cut out a sample length of at least 50 cm after the slice thickness 2−3 mm outer coils from the surface coil.

G. 3 testing

Wide-mouthed glass vessels heated in a drying Cabinet at a temperature of 120 °C for 20 min to remove the abnormal odors.

Cool at room temperature. Allowed banks before testing, purging with nitrogen.

Prepare the foil pattern of size 900 cm(30x30 cm).

Cut the sample into strips of size 1,5h30 see When testing colored foil, foil with printing or lacquer should crush the sample so that the unpainted side was on the inside, since the most likely source of smell in this case are solvents, paints, and not foil.

Place the samples in deodorized dishes.

Tightly stoppered wide-mouthed glass vessels with aluminum foil and fix the foil with a wire or a rubber ring.

Stand the cans in a drying Cabinet for 10 min at a temperature of 120 °C — for smooth foil and at 50 °C for painted, lacquered foil and foil printing.

Cool at room temperature for 10 min.

Pierce aluminum foil with a wooden stick and breathe the air in the Bank immediately after unsealing.

Inhalation should be carried out in three steps:

— fast, easy breath;

— long breath;

— a very deep breath.

Highly volatile odors is determined by the first quick breath.

G. 4 test Results

Odors define as normal and abnormal.

I think normal odor, the smell of clean appropriate material:

the annealed foil is odorless and rolling oils;

foil painted, with printing or lacquer coating is typical for this type of product odor.

In the case where the smell is assessed as abnormal, give a brief description of the sources of this odor.

The rating scale odor score:

0 — no smell;

1 — the presence of a slight smell that is different from abnormal smell;

2 — mild abnormal smell;

3 — sustainable abnormal smell or odor of solvents;

4 — strong abnormal odor or smell solvents.

Valid believe the points 0, 1 and 2.

APPENDIX e (mandatory). Method of determining wettability of the foil

APPENDIX E
(required)

This method establishes the procedure and rules of conducting the test to determine the wettability of the foil.

D. 1 Apparatus, reagents, materials

Plastic bottle-spray.

Dropper for applying drops.

Distilled water according to GOST 6709.

Ethyl alcohol (alcohol content not less than 96.6 per cent).

Solutions of ethanol in distilled water.

Classes of wetting solutions of ethanol in distilled water should be in increments of 10%, namely:

Class a: 100% distilled water — 0% ethyl alcohol.

Class: 90% distilled water 10% ethyl alcohol.

The class: 80% distilled water 20% ethanol.

Class D: 70% distilled water and 30% ethanol.

Class E: 60% distilled water 40% ethanol

etc.

D. 2 testing

2.1 General test conditions

The test is carried out at ambient temperature.

Before the test, cut off from the coil upper turns of the foil to a depth of at least 3 mm.

If the foil has a matte and shiny surfaces, the test is performed on a matte side of the foil. Test for wettability is carried out on the newly exposed surface of the foil. To re-open a new test surface. Do not carry out the re-test already on the surface of the tested sample. During the test, you must take precautions to avoid getting any liquid inside of the roll.

2.2 the Test by applying the liquid jet

Using a bottle spray is applied on the controlled surface of the foil inclined at an angle of 40° — 60°, the jet of distilled water or solutions of ethyl alcohol across the entire width of the roll. The surface of the foil along the entire width of the roll should be fully wetted with distilled water or aqueous ethanol.

2.3 Test by applying drops of fluid

With a dropper applied drops of distilled water or solutions of ethyl alcohol by weight from 40 to 80 mg on a horizontal surface of the foil across the width of the coil at a distance of 5 to 10 cm from each other. Tilt the surface of the foil at an angle of 40° — 60°.

The rate of wetting is determined by the shape of a trace of motion of a droplet left on the surface of the foil (figure D. 1).

Figure D. 1. The definition of the measure of wettability

Figure D. 1

D. 3 test Results

The wettability of the surface of the foil corresponds to the class of wettability in which distilled water or solutions of ethyl alcohol not compressed (figure D. 1, satisfactory wettability).

If there is a dispute in determining the wettability of the foil, use the solutions of ethanol in distilled water, prepared in increments of 5%.

These solutions are used in cases when you need a more accurate assessment of wettability.

ANNEX E (mandatory). A method of determining raskatyvaete foil

ANNEX E
(required)

This method establishes a test procedure for the determination of raskatyvaete foil.

The purpose of the test is to determine the extent of raskatyvaete fully annealed aluminum foil.

Ease of raskatyvaete is determined by the degree of slidenote between turns.

This test is used for aluminum foil with thickness from 0.006 to 0,050 mm.

E. 1 General test conditions

The test is carried out at ambient temperature.

Prior to testing a cut off the top coils with a controlled roll of at least 3 mm.

Hang controlled roll high enough to foil can be easily unwound by hand.

E. 2 testing

The test hung a roll of aluminum foil. Line raskatyvaete must lie in the same horizontal plane as the axis of the roll. Cut end of the foil must be located in a position corresponding to 12 hours on a clock face. Wind back the foil to a position corresponding to 3 or 9 hours on the dial (depending on which way spend the unwinding of the film roll) and let go of a foil. If the foil is spontaneously unwound to a position corresponding to 6 h, the coil is characterized by the degree of raskatyvaete A.

If the foil is spontaneously unwound, unwound free end of the foil one more complete revolution to a position corresponding to 3 or 9 hours on the clock face and release the foil. If in this case the foil is spontaneously unwound to a position corresponding to 6 h, the coil is characterized by the degree of raskatyvaete V.

In that case, if the foil is spontaneously unwound, unwound the free end of one coil and repeat the above procedure for matching the degree of raskatyvaete C. Acceptable degree of raskatyvaete think of degree A, b, C.

APPENDIX g (mandatory). Method of determining adhesion of paint coating to the surface of the foil

APP W
(required)

This method establishes the procedure for the qualitative evaluation of the breakout force of the printed image or varnish from the surface of the foil.

J. 1 Materials

Adhesive tape with peeling force of not less than 90 g/cm width.

J. 2 testing

The foil pattern selected for testing, placed on a smooth hard surface. The tape is applied to the foil pattern across the width of the coil in the direction perpendicular to the direction of machining in the manufacture of seals, leaving a free portion of the tape to grip.

Smooth the tape tight with the click of your fingers. Quickly pull (not jerking) over the free end of the tape with constant speed at an angle of 135°, but not to cause rupture of the foil or breakage of the tape. Visually inspect the tape.

The adhesion of the printing ink or varnish is estimated as follows:

And — not removed the varnish or paint;

In — on the sticky tape remains only a faint haze of glare, while not remained naked portions of the foil;

— Removes up to 10% of all paint or coatings, producing individual sections of clean foil;

D — deletes more than 10% of all paint or coatings exposing the clean foil.

AND APPLICATION (required). Rules for storage aluminum foil

THE APPLICATION AND
(required)

Aluminum foil is prone to corrosion and mechanical damage. Corrosion in the majority of cases occur under the influence of moisture, extreme temperatures and humidity and from exposure to different chemical compounds.

When careless handling of the rolls are easily clogged and the ends of the envelope surface are formed dents and nicks, preventing further free unwinding of the foil when using it. With the aim of preserving the consumer properties of aluminium foil required strict implementation of following rules.

I. 1 it is Prohibited to unload rolls of aluminum foil on the ground. In wet weather and winter time unloading the foil should be held in a special vestibule or under a canopy on a clean and dry loading dock in conditions that completely eliminates the ingress of moisture to the rolls of foil.

I. 2 it is Strictly forbidden to throw or turn over boxes with the finished products.

I. 3 In exceptional cases, when the forced delay boxes with foil in the open area should be covered with tarpaulin boxes to protect them from rain. The time of the forced storage at the open area should not exceed 5 days. Long-term storage of aluminum foil on the open areas is strictly prohibited.

I. 4 In the cold season, to avoid condensation of moisture on the surface of the rolls of foil (condensation or), may not be in a warm room and unpack the boxes with foil. Warehouse space for storage aluminum foil should be equipped with a special support facilities air temperature above the outdoor temperature, but below the temperature of the warehouse. Daily changes in temperature in the warehouse should not exceed 5 °C.

I. 5 avoid formation of coiled coils inside the condensate are not allowed to carry the rolls of foil in space temperature above 15 °C ambient temperature.

I. 6 Aluminum foil should be kept in unpacked form, in the auxiliary room to achieve the temperature of the space, then the products sent to the warehouse where kept for at least a day before unpacking.

I. 7 storage room for long-term storage, the aluminum foil must be heated, ventilated and kept clean. In the warehouse should be maintained minimum possible relative humidity, but not more than 80% and temperature not below + 5 °C.

I. 8 In the warehouse should be no access of moisture, the condensation of steam and various gases that contribute to the development of corrosion of aluminium (chlorine, smoke, ammonia, etc.).

I. 9 is Strictly forbidden storage along with aluminum foil any chemicals, actively acting on the aluminum, and materials with high humidity.

I. 10 When working with aluminum foil, you should use cotton gloves.

I. 11 to Keep the aluminum foil on the floor of the warehouse is strictly prohibited. The foil must be stored uncompressed on clean racks, upholstered in a soft material, or on racks suspended away from the heating and plumbing systems, open doors.

Shelving and rack storage foil must be made of metal or wood with a moisture content not exceeding 18%.

I. 12 Rolls of foil with a thickness of from 0.020 to 0.200 mm and width up to 200 mm is placed on the ends and put cushioning material according to GOST 7376.

The rolls of foil with a thickness of from 0.020 to 0.200 mm and width more than 200 mm is placed horizontally, separating the rows of cushioning material according to GOST 7376.

The rolls of foil with thickness less than 0.020 mm is stored only in limbo.

Allowed other cushioning materials that help to maintain the quality of foil.

I. 13 Laying on racks wet aluminum foil rolls are strictly prohibited. In case of condensation or coils should be wiped dry, especially paying attention to the ends, clean, soft material and then put on the shelves.

I. 14 Stored in the warehouse of aluminum foil shall be subjected to periodic inspection. To keep fit the aluminum foil with corrosion metal is not allowed. Corrosion foil should be immediately withdrawn.

I. 15 subject to the above storage conditions the manufacturer guarantees the preservation of all consumer properties of soft (annealed) foil for 6 months and hard (cold-rolled) for 12 months from the date of issue of the document about quality (3.1 of this standard).

ANNEX K (informative). Bibliography

APP TO
(reference)

[1] GN 2.3.3.972−2000* Maximum permissible quantities of chemical substances emitted from materials contacting with food products
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* Operate on the territory of the Russian Federation.


(Amendment. ICS N 9−2004).